反应条件
1: Clemmensen reduction
2: 2.) NaBH4 / 1.) 120 deg C, 2.5 h, 2.) CHCl3, EtOH, r.t., 8 h
3: 1.) H3BO3, 2.) NaBH4 / 1.) CH3OH, H2O, r.t.
4: 16.4 percent / KI / Ni(PPh3)2Cl2-Zn-PPh3 / dimethylformamide / 55 °C
View Scheme
参考文献
Kihara, Masaru; Itoh, Joji; Iguchi, Seiichiro; Imakura, Yasuhiro; Kobayashi, Shigeru
Journal of Chemical Research, Miniprint, 1988 , # 1 p. 157 - 177
