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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
820975-37-9
合成路线
(共 4 条)
820975-38-0
→
反应条件
820975-37-9
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane 4 h; RefluxIrradiation;
参考文献
Mesangeau, Christophe; Fraise, Mikael; Delagrange, Philippe; Caignard, Daniel Henri; Boutin, Jean Albert; Berthelot, Pascal; Yous, Said
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 5 p. 1835 - 1840
371-42-6
对氟苯硫酚
→
反应条件
820975-37-9
反应条件
1: sodium hydroxide / water / 1 h / 0 °C 2: polyphosphoric acid / 1 h / 80 °C 3: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux; Irradiation View Scheme
参考文献
Mesangeau, Christophe; Fraise, Mikael; Delagrange, Philippe; Caignard, Daniel Henri; Boutin, Jean Albert; Berthelot, Pascal; Yous, Said
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 5 p. 1835 - 1840
2968-13-0
(4-氟苯基硫)丙酮
→
反应条件
820975-37-9
反应条件
1: polyphosphoric acid / 1 h / 80 °C 2: N-bromosuccinmide; dibenzoyl peroxide / tetrachloromethane / 4 h / Reflux; Irradiation View Scheme
参考文献
Mesangeau, Christophe; Fraise, Mikael; Delagrange, Philippe; Caignard, Daniel Henri; Boutin, Jean Albert; Berthelot, Pascal; Yous, Said
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 5 p. 1835 - 1840
773837-37-9
+
820975-37-9
→
反应条件
820975-39-1
反应条件
in dimethyl sulfoxide T=20°C; 1 h;
参考文献
Mesangeau, Christophe; Fraise, Mikael; Delagrange, Philippe; Caignard, Daniel Henri; Boutin, Jean Albert; Berthelot, Pascal; Yous, Said
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 5 p. 1835 - 1840