1,4-二氯-2-丁炔合成路线 （共 101 条）
反应条件
potassium hydroxide in tetrahydrofuran 5 h;
参考文献
Kerton, Francesca M.; Mohmand, G. Farouq; Tersteegen, Adrian; Thiel, Markus; Went, Michael J.
Journal of Organometallic Chemistry, 1996 , vol. 519, # 1-2 p. 177 - 184
反应条件
tetrachloromethane; chlorine
参考文献
Wille et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 591, p. 177,186
Full Text Show Details
Schostakowskii; Schmonina
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 109;engl.Ausg.S.106
反应条件
in N,N-dimethyl-formamide T=0°C; 4 h; Heating / reflux;
参考文献
AGENCY FOR SCIENCE, TECHNOLOGY AND RESEARCH
Patent: WO2007/58630 A1, 2007 ;
Location in patent: Page/Page column 22-23 ;
反应条件
N,N-dimethyl-formamide
参考文献
Fraser; Raphael
Journal of the Chemical Society, 1952 , p. 226
反应条件
tetrachloromethane; bromine
参考文献
Akhrem,A.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1960 , p. 654 - 661
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1960 , # 4 p. 693 - 702
参考文献
Valette
Annales de Chimie (Cachan, France), 1948 , vol. <12>3, p. 674
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1946 , vol. 223, p. 908
反应条件
copper(I) bromide in tetrahydrofuran T=-20 - 0°C;
参考文献
Brandsma, Lambert; Meijer, Johnny; Verkruijsse, Herman D.; Bokkers, Gysbertus; Duisenberg, Albert J. M.; Kroon, Jan
Journal of the Chemical Society, Chemical Communications, 1980 , # 19 p. 922 - 923
反应条件
sodium carbonate in benzene T=65 - 70°C; 16 h; Inert atmosphere;
参考文献
Ionovation GmbH; Rosemeyer, Helmut; Malecki, Edith; Korneev, Sergei; Werz, Emma; Gall, Karsten
Patent: EP2712869 A1, 2014 ;
Location in patent: Paragraph 0162 ;
反应条件
hydrazine hydrate; potassium hydroxide T=25 - 50°C;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 45, # 8 p. 1009 - 1010
反应条件
borane; acetic acid multistep reaction, stereospecificity, various alkenes; Product distribution;
参考文献
Hoshi, Masayuki; Arase, Akira
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 22 p. 2693 - 2700
