chloro-trimethyl-silane; iodine; magnesium in tetrahydrofuran 56 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 50, # 25 p. 5193 - 5199
1: With AlCl3, aluminium chloride in tetrahydrofuran T=0 - 20°C; 1 h; 2: With FeCl2(TMS-SciOPP) in tetrahydrofuran T=80°C; 12 h; 3: With hydrogenchloride in tetrahydrofuran; water T=0 - 20°C; 3 h;
参考文献
Chemical Communications, , vol. 48, # 75 p. 9376 - 9378
1: in tetrahydrofuran T=0 - 20°C; 1 h; 2: With FeCl2(TMS-SciOPP) in tetrahydrofuran T=80°C; 12 h; 3: With hydrogenchloride in tetrahydrofuran; water T=0 - 20°C; 3 h;
参考文献
Chemical Communications, , vol. 48, # 75 p. 9376 - 9378
1: in tetrahydrofuran T=0 - 20°C; 1 h; 2: With FeCl2(TMS-SciOPP) in tetrahydrofuran T=80°C; 12 h; 3: With hydrogenchloride in tetrahydrofuran; water T=0 - 20°C; 3 h;
参考文献
Chemical Communications, , vol. 48, # 75 p. 9376 - 9378
