反应条件
1: 3',4'-(methylenedioxy)acetophenone With sodium ethanolate in diethyl ether
T=20°C; 0.25 h;
2: formic acid ethyl ester in diethyl ether
T=20°C; 3 h;
3: ethyl bromide in diethyl ether
T=20°C; 24 h; Further stages.;
参考文献
Stern, Eric; Muccioli, Giulio G.; Bosier, Barbara; Hamtiaux, Laurie; Millet, Regis; Poupaert, Jacques H.; Henichart, Jean-Pierre; Depreux, Patrick; Goossens, Jean-Francois; Lambert, Didier M.
Journal of Medicinal Chemistry, 2007 , vol. 50, # 22 p. 5471 - 5484
