in water an excess of Ag2CO3 is added (stirring) to a soln. of HN(SO2CF3)2 in water; mixt. heated up to about 65°C; filtered and concd.; water removed under vac.; dried at about 80°C for 6 h; dissolved in diethyl ether, stirred for ca 2 h and filtered;solvent removed under vac.; elem. anal.;
参考文献
Vij, Ashwani; Zheng, Yuan Y.; Kirchmeier, Robert L.; Shreeve, Jean'ne M.
Inorganic Chemistry, 1994 , vol. 33, p. 3281 - 3288
