反应条件
1: ZnI2 / CH2Cl2 / 65 h / Ambient temperature
2: 94 percent / HCl / 16 h / 5 °C
3: 83 percent / Et3N / tetrahydrofuran / 1 h / 0 - 5 °C
4: dimethylsulfoxide; methanol / 1.) 20 deg C, 16 h, 2.) 106 deg C, 5 h
View Scheme
参考文献
Schnur; Morville
Journal of Medicinal Chemistry, 1986 , vol. 29, # 5 p. 770 - 778
