1,2-o-二十八基-sn-甘油合成路线 （共 5 条）
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
12 h;
参考文献
Figueroa-Perez, Santiago; Verez-Bencomo, Vicente
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 6 p. 851 - 868
反应条件
titanium tetrachloride in dichloromethane
T=0°C; 1 h;
参考文献
Yamauchi, Kiyoshi; Hihara, Mitsuyoshi; Kinoshita, Masayoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 2169 - 2172
反应条件
titanium tetrachloride in dichloromethane
T=0°C; 1 h;
参考文献
Yamauchi, Kiyoshi; Hihara, Mitsuyoshi; Kinoshita, Masayoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 2169 - 2172
反应条件
1: 1.) sodiumhydride / 1.) THF, oil, 30 min, room temp., 2.) 190-200 deg C
2: 61 percent / titanium tetrachloride / CH2Cl2 / 1 h / 0 °C
View Scheme
参考文献
Yamauchi, Kiyoshi; Hihara, Mitsuyoshi; Kinoshita, Masayoshi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, p. 2169 - 2172
反应条件
1: 77.1 percent / KOH / benzene / 12 h / Heating
2: 97 percent / H2 / Pd/C / ethyl acetate / 12 h
View Scheme
参考文献
Figueroa-Perez, Santiago; Verez-Bencomo, Vicente
Journal of Carbohydrate Chemistry, 1998 , vol. 17, # 6 p. 851 - 868
