1: n-octanethiol With sodium salt of phosphorous acid in N,N-dimethyl-formamide
0.25 h;
2: monobromotrifluoromethane With hydroxymethanesulfinic acid sodium salt in N,N-dimethyl-formamide
T=20°C; P=3375.27 Torr; 8 h; Title compound not separated from byproducts;
参考文献
Magnier, Emmanuel; Wakselman, Claude
Synthesis, 2003 , # 4 p. 565 - 569