反应条件
1: BH3*Me2S / tetrahydrofuran / 3 h / 0 °C
2: 1.) PPh3, diisopropyl diazodicarboxylate, Zn(N3)2*2 pyridine, 2.) nBu3SnH, AIBN / 1.) toluene, room temperature, 24 h, 2.) benzene, reflux, 23 h
View Scheme
参考文献
De Mesmaeker, Alain; Wendeborn, Sebastian; Jouanno, Chantal; Fritsch, Valerie; Wolf, Romain M.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 14 p. 1869 - 1874
