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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82203-83-6
合成路线
（共 17 条）
887144-97-0
3,3-二甲基-1-(三氟甲基)-1,2-苯并碘氧杂戊环
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
82203-83-6
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium hydrogencarbonate in dichloromethane T=20°C; 18 h; Inert atmosphere;
参考文献
Weng, Zhiqiang; Li, Huaifeng; He, Weiming; Yao, Liang-Feng; Tan, Jianwei; Chen, Jinfa; Yuan, Yaofeng; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 11 p. 2527 - 2531
→
反应条件
82203-83-6
反应条件
tert.-butylhydroperoxide; sodium hydrogencarbonate; copper(l) chloride in methanol; dichloromethane; water T=0 - 20°C;
参考文献
Dubbaka, Srinivas Reddy; Nizalapur, Shashidhar; Atthunuri, Azmi Reddy; Salla, Manohar; Mathew, Thresen
Tetrahedron, 2014 , vol. 70, # 12 p. 2118 - 2121
118968-67-5
→
反应条件
82203-83-6
反应条件
potassium hydroxide in dimethyl sulfoxide Ambient temperature;
参考文献
Meazza, G.; Zanardi, G.
Journal of Fluorine Chemistry, 1991 , vol. 55, # 2 p. 199 - 206
1514-82-5
2-溴-3,3,3-三氟丙烯
+
696-62-8
4-碘苯甲醚
→
反应条件
82203-83-6
反应条件
1: 2-Bromo-3,3,3-trifluoro-propene With ZnCl2*TMEDA; lithium diisopropyl amide in tetrahydrofuran; hexane T=-78 - 20°C; 1 h; 2: para-iodoanisole With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane 6 h; Heating;
参考文献
Konno, Tsutomu; Chae, Jungha; Kanda, Masashi; Nagai, Go; Tamura, Kazushige; Ishihara, Takashi; Yamanaka, Hiroki
Tetrahedron, 2003 , vol. 59, # 38 p. 7571 - 7580
→
反应条件
82203-83-6
反应条件
[2,2']bipyridinyl; copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide T=60°C; 6 h;
参考文献
Wang, Xiaoping; Lin, Jinhong; Zhang, Chengpan; Xiao, Jichang; Zheng, Xing
Chinese Journal of Chemistry, 2013 , vol. 31, # 7 p. 915 - 920
77152-08-0
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
82203-83-6
反应条件
N,N,N',N,-tetramethylethylenediamine; triethyl amine hydrochloride in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Serizawa, Hiroki; Aikawa, Kohsuke; Mikami, Koichi
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17692 - 17697
81290-20-2
(三氟甲基)三甲基硅烷
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
82203-83-6
反应条件
potassium fluoride; copper(l) iodide; 1,10-phenanthroline in N,N-dimethyl-formamide T=100°C; 6 h;
参考文献
Chu, Lingling; Qing, Feng-Ling
Journal of the American Chemical Society, 2010 , vol. 132, # 21 p. 7262 - 7263
→
反应条件
82203-83-6
反应条件
copper(I) isothiocyanate in acetonitrile T=20°C; 16 h;
参考文献
Zheng, Huidong; Huang, Yuanyuan; Wang, Zhiwei; Li, Huaifeng; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron Letters, 2012 , vol. 53, # 49 p. 6646 - 6649
82203-88-1
→
反应条件
82203-83-6
反应条件
T=410°C; P=10 Torr;
参考文献
Kobayashi, Yoshiro; Yamashita, Toshinori; Takahashi, Katsuhiro; Kuroda, Hisashi; Kumadaki, Itsumaro
Chemical and Pharmaceutical Bulletin, 1984 , vol. 32, # 11 p. 4402 - 4409
1058685-73-6
+
768-60-5
4-乙炔基苯甲醚
→
反应条件
82203-83-6
反应条件
1: 4-ethynyl-1-methoxy-benzene With n-butyllithium in tetrahydrofuran T=0°C; 0.25 h; Inert atmosphere; 2: N,N-(dimethylamino)-S-phenyl-S-trifluoromethyloxosulfonium trifluoromethanesulfonate in tetrahydrofuran T=-78 - 20°C; 2 h; Inert atmosphere;
参考文献
Urban, Celine; Cadoret, Frederic; Blazejewski, Jean-Claude; Magnier, Emmanuel
European Journal of Organic Chemistry, 2011 , # 25 p. 4862 - 4867
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