2-(羟基甲基)-6-(2-硝基咪唑-1-基)-3,6-二氢-2H-吡喃-3-醇合成路线 （共 3 条）
参考文献
Sakaguchi, Masakazu; Larroquette, Cynthia A.; Agrawal, Krishna C.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 1 p. 20 - 24
反应条件
1: 5.2 percent / SnCl4 / CH2Cl2 / 0.75 h / 60 - 70 °C
2: 66.3 percent / sat. methanol. NH3 / 0 °C
View Scheme
参考文献
Sakaguchi, Masakazu; Larroquette, Cynthia A.; Agrawal, Krishna C.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 1 p. 20 - 24
反应条件
1: 2.) ZnCl2 / 1.) from 90 to 100 deg C, 10 min, vacuum, 2.) from 140 to 160 deg C, 45 min, vacuum
2: 66.3 percent / sat. methanol. NH3 / 0 °C
View Scheme
参考文献
Sakaguchi, Masakazu; Larroquette, Cynthia A.; Agrawal, Krishna C.
Journal of Medicinal Chemistry, 1983 , vol. 26, # 1 p. 20 - 24
