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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82238-29-7
合成路线
（共 11 条）
82238-23-1
→
反应条件
82238-29-7
反应条件
1,4-diaza-bicyclo[2.2.2]octane in benzene Ambient temperature;
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Tomimatsu, Kiminori
Tetrahedron Letters, 1982 , vol. 23, # 8 p. 901 - 904
82238-25-3
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature 2: 83.8 percent / diethyl ether; benzene / 3 h / Heating 3: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-T 4: 94 percent / DABCO / benzene / 24 h / Ambient temperature View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
30673-29-1
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 2: acetonitrile / 3 h / Ambient temperature 3: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
23974-72-3
→
反应条件
82238-29-7
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: acetonitrile / 3 h / Ambient temperature 6: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
89-98-5
2-氯苯甲醛
→
反应条件
82238-29-7
反应条件
1: 86.1 percent / dimethylformamide / 4 h / 120 °C 2: 98.7 percent / diethyl ether / 1 h / Heating 3: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 4: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 5: acetonitrile / 3 h / Ambient temperature 6: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-84-4
→
反应条件
82238-29-7
反应条件
1: 98.7 percent / diethyl ether / 1 h / Heating 2: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 3: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 4: acetonitrile / 3 h / Ambient temperature 5: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
88048-85-5
→
反应条件
82238-29-7
反应条件
1: 79.6 percent / 80percent H2SO4 / 0.5 h / 95 °C 2: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 3: acetonitrile / 3 h / Ambient temperature 4: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
80-16-0
N-氯-苯磺酰胺
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature 3: 100 percent / 1,4-diazabicyclo<2.2.2>octane / benzene / Ambient temperature; also N-benzenesulfonyl substituted selenilimine investigated View Scheme
参考文献
Hori, Mikio; Kataoka, Tadashi; Shimizu, Hiroshi; Tomimatsu, Kiminori
Tetrahedron Letters, 1982 , vol. 23, # 8 p. 901 - 904
127-65-1
氯胺T
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-T 2: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
127-52-6
氯胺 B
→
反应条件
82238-29-7
反应条件
1: acetonitrile / 3 h / Ambient temperature; 1 eq. chloramine-B 2: acetonitrile / 3 h / Ambient temperature 3: 98 percent / toluene / 6 h / Heating View Scheme
参考文献
Tomimatsu, Kiminori; Kataoka, Tadashi; Shimizu, Hiroshi; Hori, Mikio
Phosphorus and Sulfur and the Related Elements, 1983 , vol. 16, p. 97 - 110
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