Dehand, J.; Mauro, A.; Ossor, H.; Pfeffer, M.; Santos, R. H. De A.; Lechat, J. R.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 537 - 550
CO in toluene
CO bubbled into toluene soln. of educt;
参考文献
Dehand, J.; Mauro, A.; Ossor, H.; Pfeffer, M.; Santos, R. H. De A.; Lechat, J. R.
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. 537 - 550
Artz, Steven P.; deGrandpre, Mark P.; Cram, Donald J.
Journal of Organic Chemistry, 1985 , vol. 50, # 9 p. 1486 - 1496
→
反应条件
in toluene
under N2; a toluene soln. of Pd-complex was added to equimolar amt. of Hg(O2CMe)2, soln. refluxed for 15 min,; addn. of pentane, soln. left overnight at -20 ° C, yellow crystals, elem. anal.;
参考文献
Wehman, Erik; Koten, Gerard van; Jastrzebski, Johann T. B. H.; Ossor, Houssaine; Pfeffer, Michel
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1988 , p. 2975 - 2982