3,6-二甲基-2-吡啶胺合成路线 （共 3 条）
反应条件
1: 87 percent / PCl5 / CHCl3 / 3 h / Heating 2: NaH, N-methylaniline / Heating View Scheme
参考文献
Mahadevan,Indumathy; Rasmussen, Malcolm
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 359 - 367
反应条件
1: 87 percent / PCl5 / CHCl3 / 3 h / Heating 2: NaH, N-methylaniline / Heating 3: 14 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 20 h / Ambient temperature 4: 1.) HNO3, trifluoroacetic acid, 2.) PCl3, 3.) NaH View Scheme
参考文献
Meade, Eric A.; Beauchamp, Lilia M.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 2 p. 303 - 308
反应条件
1: 87 percent / PCl5 / CHCl3 / 3 h / Heating 2: NaH, N-methylaniline / Heating 3: 14 percent / m-chloroperoxybenzoic acid / CH2Cl2 / 20 h / Ambient temperature View Scheme
参考文献
Meade, Eric A.; Beauchamp, Lilia M.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 2 p. 303 - 308
