in dichloromethane byproducts: C6H5NH2; under N2, to CH2Cl2 simultaneously added dropwise MeBBr2 (0.1 mole) and0.1 mole of mixt. of O(SiMe3)2 (0.066 mole) and PhN(SiMe3)2 (0.033 mole) at room temp., refluxed for 6 h; evapd., sepd. by distn.;
参考文献
Oesterle, Rainer; Maringgele, Walter; Meller, Anton
Journal of Organometallic Chemistry, 1985 , vol. 284, p. 281 - 290