反应条件
1: 1.) diisopropylamine, n-BuLi / 1.) THF, 45 min, -78 deg C
2: 26 percent / TiCl4 / CH2Cl2 / 1.) 8 h, -78 deg C, 2.) 39,5 h, room temp.
View Scheme
参考文献
Albaugh-Robertson, Pamela; Katzenellenbogen, John A.
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5288 - 5302
