苄基(1-氧代-2-丙基)氨基甲酸酯合成路线 （共 3 条）
反应条件
1: potassium fluoride / isopropyl alcohol / 8 h / 0 - 20 °C 2: 4-(N,N-dimethlyamino)pyridine / diethyl ether / 2 h / 25 °C / |Inert atmosphere 3: sodium tetrahydroborate / ethanol / 2 h / 0 °C / |Inert atmosphere 4: sodium nitrite; acetic acid / dimethyl sulfoxide / 20 h / 40 °C / |Inert atmosphere View Scheme
参考文献
Sleebs, Brad E.; Nguyen, Nghi H.; Hughes, Andrew B.
Synlett, 2013 , vol. 24, # 6 art. no. ST-2012-B0741-L, p. 747 - 751
反应条件
sodium tetrahydroborate
参考文献
McDonald, Richard I.; Wong, Gene W.; Neupane, Ram P.; Stahl, Shannon S.; Landis, Clark R.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14027 - 14029
反应条件
sodium tetrahydroborate
参考文献
McDonald, Richard I.; Wong, Gene W.; Neupane, Ram P.; Stahl, Shannon S.; Landis, Clark R.
Journal of the American Chemical Society, 2010 , vol. 132, # 40 p. 14027 - 14029
