(R)-2-(叔丁氧羰基氨基)丙醛合成路线 （共 9 条）
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; trichloroisocyanuric acid in dichloromethane
T=0 - 20°C; 0.25 h;
参考文献
Yao, Haoyi; Yamamoto, Kana
Chemistry - An Asian Journal, 2012 , vol. 7, # 7 p. 1542 - 1545
反应条件
diisobutylaluminium hydride in tetrahydrofuran; hexane
T=-78°C; 0.333333 h;
参考文献
Chakravarty, Prasun K.; Greenlee, William J.; Parsons, William H.; Patchett, Arthur A.; Combs, Patricia; et al.
Journal of Medicinal Chemistry, 1989 , vol. 32, # 8 p. 1886 - 1890
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0°C; 1 h;
参考文献
Boger, Dale L.; Menezes, Royce F.
Journal of Organic Chemistry, 1992 , vol. 57, # 16 p. 4331 - 4333
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Boger, Dale L.; Colletti, Steven L.; Honda, Takeshi; Menezes, Royce F.
Journal of the American Chemical Society, 1994 , vol. 116, # 13 p. 5607 - 5618
反应条件
1: EtN=C=N(CH2)3NMe2*HCl; iPr2NEt / tetrahydrofuran; dimethylformamide
2: LiAlH4 / diethyl ether / 0 °C
View Scheme
参考文献
Nakano, Ayako; Takahashi, Keisuke; Ishihara, Jun; Hatakeyama, Susumi
Organic Letters, 2006 , vol. 8, # 23 p. 5357 - 5360
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=-20°C;
参考文献
Narita, Masatoshi; Otsuka, Masami; Kobayashi, Susumu; Ohno, Masaji
Tetrahedron Letters, 1982 , vol. 23, # 5 p. 525 - 528
参考文献
General Foods Corporation
Patent: US4603012 A1, 1986 ;
反应条件
1: 19.39 g / triethylamine / CH2Cl2; methanol / 1.) room temperature, 1 h, 2.) 35 deg C, overnight
2: 11.06 g / diisobutylaluminum hydride / toluene / 0.25 h
View Scheme
参考文献
Pihko, Petri M.; Koskinen, Ari M. P.
Journal of Organic Chemistry, 1998 , vol. 63, # 1 p. 92 - 98
反应条件
1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in ethyl acetate
2 h; Heating; Title compound not separated from byproducts;
参考文献
Ocejo, Marta; Vicario, Jose L.; Badia, Dolores; Carrillo, Luisa; Reyes, Efraim
Synlett, 2005 , # 13 art. no. G12505ST, p. 2110 - 2112
反应条件
Yield given. Multistep reaction;
参考文献
Itaya, Taisuke; Fujii, Tozo; Evidente, Antonio; Randazzo, Giacomino; Surico, Giuseppe; Iacobellis, Nicola S.
Tetrahedron Letters, 1986 , vol. 27, # 52 p. 6349 - 6352
