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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82366-98-1
合成路线
（共 16 条）
3141-27-3
2,5-二溴噻吩
+
5720-05-8
4-甲基苯硼酸
→
反应条件
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine in tetrahydrofuran T=20°C; Suzuki coupling; 6 h;
参考文献
Dong, Cheng-Guo; Hu, Qiao-Sheng
Journal of the American Chemical Society, 2005 , vol. 127, # 28 p. 10006 - 10007
33491-05-3
→
反应条件
82366-98-1
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in N,N-dimethyl-formamide T=70°C; 6 h; regioselective reaction;
参考文献
Jiang, Huanfeng; Zeng, Wei; Li, Yibiao; Wu, Wanqing; Huang, Liangbing; Fu, Wei
Journal of Organic Chemistry, 2012 , vol. 77, # 11 p. 5179 - 5183
16939-04-1
(4-噻吩-2-苯基)甲醇
+
106-38-7
对溴甲苯
→
反应条件
82366-98-1
反应条件
C40H36N2O2Pd(2+)*2C2H4O2; potassium carbonate; 2,2,2-trimethylacetic acid in N,N-dimethyl acetamide T=100°C; 24 h; Inert atmosphereSchlenk technique; regioselective reaction;
参考文献
Li, Yabo; Wang, Jingran; Huang, Mengmeng; Wang, Zhiwei; Wu, Yusheng; Wu, Yangjie
Journal of Organic Chemistry, 2014 , vol. 79, # 7 p. 2890 - 2897
13145-56-7
→
反应条件
82366-98-1
反应条件
Lawesson's reagent in toluene Heating;
参考文献
Shridhar, D. R.; Jogibhukta, M.; Shanthan, Rao P.; Handa, Vijay K.
Synthesis, 1982 , # 12 p. 1061 - 1062
128407-55-6
→
反应条件
1020209-01-1
+
82366-98-1
反应条件
Lawesson's reagent in toluene Paal-Knorr cyclization; Heating;
参考文献
Yin, Guodong; Wang, Zihua; Chen, Aihua; Gao, Meng; Wu, Anxin; Pan, Yuanjiang
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3377 - 3383
→
反应条件
82366-98-1
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; silver(l) oxide in methanol T=20°C; Suzuki-Miyaura cross- coupling; Inert atmosphere;
参考文献
Botteselle, Giancarlo V.; Hough, Thomas L. S.; Venturoso, Raphael C.; Cella, Rodrigo; Vieira, Adriano S.; Stefani, Helio A.
Australian Journal of Chemistry, 2008 , vol. 61, # 11 p. 870 - 873
3141-27-3
2,5-二溴噻吩
+
4294-57-9
对甲苯基溴化镁
→
反应条件
82366-98-1
反应条件
Ni(dppp)Cl2 in tetrahydrofuran
参考文献
Sheina, Elena E.; Liu, Jinsong; Lovu, Mihaela Corina; Laird, Darin W.; McCullough, Richard D.
Macromolecules, 2004 , vol. 37, # 10 p. 3526 - 3528
22666-07-5
→
反应条件
82366-98-1
反应条件
1: 14.35 g / NaOH / ethanol / 6 h / Heating 2: 40.5 percent / KOH / dimethylformamide / 2 h / 46 °C 3: 61 percent / HCl(gas) / dioxane / 2 h View Scheme
参考文献
Schroth, Werner; Dunger, Simona; Billig, Frank; Spitzner, Roland; Herzschuh, Rainer; Vogt, Almut; Jende, Thomas; Israel, Gunter; Barche, Jens; Stroehl, Dieter; Sieler, Joachim
Tetrahedron, 1996 , vol. 52, # 39 p. 12677 - 12698
22666-07-5
→
反应条件
82366-98-1
+
1426938-83-1
反应条件
in N,N-dimethyl-formamide T=150°C; 2 h; Schlenk techniqueInert atmosphere;
参考文献
Tang, Jialiang; Ming, Ling; Zhao, Xiaoming
Synthesis (Germany), 2013 , vol. 45, # 12 art. no. SS-2013-H0207-OP, p. 1713 - 1718
5720-05-8
4-甲基苯硼酸
→
反应条件
82366-98-1
反应条件
1: C40H36N2O2Pd(2+)*2C2H4O2; potassium hydroxide / ethanol / 78 °C / |Inert atmosphere; |Schlenk technique 2: C40H36N2O2Pd(2+)*2C2H4O2; potassium carbonate; 2,2,2-trimethylacetic acid / N,N-dimethyl acetamide / 24 h / 100 °C / |Inert atmosphere; |Schlenk technique View Scheme
参考文献
Li, Yabo; Wang, Jingran; Huang, Mengmeng; Wang, Zhiwei; Wu, Yusheng; Wu, Yangjie
Journal of Organic Chemistry, 2014 , vol. 79, # 7 p. 2890 - 2897
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