3-(二乙氨基)-1,5-二氢-2,4,3-苯并二噁磷杂庚英合成路线 （共 3 条）
反应条件
triethylamine in tetrahydrofuran; diethyl ether T=-78 - 20°C;
参考文献
Journal of Organometalic Chemistry, , vol. 646, # 1-2 p. 239 - 246
参考文献
Arbuzov, B. A.; Kadyrov, R. A.; Klochkov, V. V.; Arshinova, R. P.; Aganov, A. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 3 p. 520 - 525
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 3 p. 588 - 593
反应条件
1: 1H-tetrazole / CH2Cl2 / 0.25 h / Ambient temperature 2: 89 percent / PyHBr3, Et3N, molecular sieves / CH2Cl2 / a) -40 deg C, 15 min, b) r.t., 10 min View Scheme
参考文献
Watanabe, Yutaka; Komoda, Yasunobu; Ozaki, Shoichiro
Tetrahedron Letters, 1992 , vol. 33, # 10 p. 1313 - 1316
