T=650°C; beim Leiten durch ein verzinntes Eisenrohr;

potassium permanganate in sodium hydroxide Heatingovernight;

暂无反应条件数据

hydrogen; platinum(IV) oxide in tetrahydrofuran P=1034.3 Torr;

1: 1 percent Chromat. / TsOH / benzene / 0.3 h / Heating 2: Pd/C / 4 h / 320 °C View Scheme

1: 90 percent Chromat. / TsOH / benzene / 11 h / Heating 2: Pd/C / 4 h / 320 °C View Scheme

1: 93 percent / AlCl3 / CS2 / 3 h / Heating 2: 98 percent / NaBH4 / ethanol / 2 h / 25 °C 3: 92 percent / p-toluenesulfonic acid*H2O / benzene / 1 h / Heating 4: 96 percent / NiCl2<dppp>2 / diethyl ether / 22 h / Heating 5: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme

1: 89 percent / KOH / acetic acid; H2O; tetrahydrofuran / 12 h / 25 °C 2: 81 percent / 165 °C 3: thionyl chloride / 0.75 h / Heating 4: 93 percent / AlCl3 / CS2 / 3 h / Heating 5: 98 percent / NaBH4 / ethanol / 2 h / 25 °C 6: 92 percent / p-toluenesulfonic acid*H2O / benzene / 1 h / Heating 7: 96 percent / NiCl2<dppp>2 / diethyl ether / 22 h / Heating 8: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme

1: 98 percent / NaBH4 / ethanol / 2 h / 25 °C 2: 92 percent / p-toluenesulfonic acid*H2O / benzene / 1 h / Heating 3: 96 percent / NiCl2<dppp>2 / diethyl ether / 22 h / Heating 4: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme

1: thionyl chloride / 0.75 h / Heating 2: 93 percent / AlCl3 / CS2 / 3 h / Heating 3: 98 percent / NaBH4 / ethanol / 2 h / 25 °C 4: 92 percent / p-toluenesulfonic acid*H2O / benzene / 1 h / Heating 5: 96 percent / NiCl2<dppp>2 / diethyl ether / 22 h / Heating 6: 98 percent / H2 / PtO2 / tetrahydrofuran / 1034.3 Torr View Scheme