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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
824-43-1
合成路线
（共 51 条）
141-43-5
乙醇胺
→
反应条件
824431-19-8
反应条件
sodium carbonate in acetonitrile 5 h; Reflux;
参考文献
Harit, Tariq; Malek, Fouad; Bali, Brahim El; Khan, Ajmal; Dalvandi, Kourosh; Marasini, Bishnu P.; Noreen, Shagufta; Malik, Rizwana; Choudhary, M. Iqbal; Khan, Sadia
Medicinal Chemistry Research, 2012 , vol. 21, # 10 p. 2772 - 2778,7
5744-51-4
1,5-二甲基-1H-吡唑-3-甲酸乙酯
→
反应条件
824431-19-8
反应条件
1: lithium aluminium tetrahydride 2: thionyl chloride 3: sodium carbonate / acetonitrile / 5 h / |Reflux View Scheme
参考文献
Harit, Tariq; Malek, Fouad; Bali, Brahim El; Khan, Ajmal; Dalvandi, Kourosh; Marasini, Bishnu P.; Noreen, Shagufta; Malik, Rizwana; Choudhary, M. Iqbal; Khan, Sadia
Medicinal Chemistry Research, 2012 , vol. 21, # 10 p. 2772 - 2778,7
4027-57-0
3-甲基吡唑-5-甲酸乙酯
→
反应条件
824431-19-8
反应条件
1: potassium tert-butylate 2: lithium aluminium tetrahydride 3: thionyl chloride 4: sodium carbonate / acetonitrile / 5 h / |Reflux View Scheme
参考文献
Harit, Tariq; Malek, Fouad; Bali, Brahim El; Khan, Ajmal; Dalvandi, Kourosh; Marasini, Bishnu P.; Noreen, Shagufta; Malik, Rizwana; Choudhary, M. Iqbal; Khan, Sadia
Medicinal Chemistry Research, 2012 , vol. 21, # 10 p. 2772 - 2778,7
18922-04-8
6-碘-1-己烯
+
1119-60-4
6-庚烯酸
→
反应条件
824431-34-7
反应条件
1: 4-(Propyl-2-ene)butyric acid With N,N'-dimethyl-N,N'-propyleneurea; n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=20°C; 1 h; 2: 6-iodohexene in tetrahydrofuran; hexane T=20°C; 2 h;
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
1119-60-4
6-庚烯酸
+
638-45-9
1-碘己烷
→
反应条件
824431-37-0
反应条件
1: 4-(Propyl-2-ene)butyric acid With N,N'-dimethyl-N,N'-propyleneurea; n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=20°C; 1 h; 2: 1-iodo-n-hexane in tetrahydrofuran; hexane T=20°C; 2 h;
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
2033-24-1
米氏酸
+
910788-16-8
→
反应条件
824431-40-5
反应条件
caesium carbonate in acetonitrile T=20°C; 72 h;
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
14371-10-9
桂皮醛
→
反应条件
824431-40-5
反应条件
1: 71 percent / BH3*HNMe2 / methanol / 3 h / 20 °C 2: 90 percent / 1.5 h / 170 °C / microwave irradiation 3: 100 percent / DIBALH / tetrahydrofuran; CH2Cl2 / 4 h / -78 °C 4: 89 percent / I2; PPh3; imidazole / CH2Cl2 / 0 - 20 °C 5: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C View Scheme
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
72651-96-8
→
反应条件
824431-40-5
反应条件
1: 90 percent / 1.5 h / 170 °C / microwave irradiation 2: 100 percent / DIBALH / tetrahydrofuran; CH2Cl2 / 4 h / -78 °C 3: 89 percent / I2; PPh3; imidazole / CH2Cl2 / 0 - 20 °C 4: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C View Scheme
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
22768-07-6
→
反应条件
824431-40-5
反应条件
1: 100 percent / DIBALH / tetrahydrofuran; CH2Cl2 / 4 h / -78 °C 2: 89 percent / I2; PPh3; imidazole / CH2Cl2 / 0 - 20 °C 3: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C View Scheme
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
13159-16-5
5-苯基戊-4-烯基-1-醇
→
反应条件
824431-40-5
反应条件
1: 89 percent / I2; PPh3; imidazole / CH2Cl2 / 0 - 20 °C 2: 47 percent / cesium carbonate / acetonitrile / 72 h / 20 °C View Scheme
参考文献
Belanger, Guillaume; Levesque, Francois; Paquet, Julie; Barbe, Guillaume
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 291 - 296
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