反应条件
1: methanol / 19 h / Heating 2: 1.) BuLi / 1.) THF, a.) -78 deg C, 20 min, b.) RT, 20 min, 2.) THF, from -78 deg C to RT 3: 1.) BuLi, 2.) CCl4 / 1.) THF, -78 deg C, 2.) THF, 20 min 4: 79 percent / AgClO4, CF3COOH / H2O / 1 h / Heating View Scheme
参考文献
Kotake, Hiroshi; Inomata, Katsuhiko; Kinoshita, Hideki; Sakamoto, Yasuko; Kaneto, Yoko
Bulletin of the Chemical Society of Japan, 1980 , vol. 53, # 10 p. 3027 - 3028
