1: 1,5-dihydroxypentane With sodium hydride in tetrahydrofuran 3 h; Heating; 2: p-methoxybenzyl chloride With tetra-(n-butyl)ammonium iodide in tetrahydrofuran 15 h;
参考文献
Smith III, Amos B.; Fox, Richard J.; Vanecko, John A.
Organic Letters, 2005 , vol. 7, # 14 p. 3099 - 3102
1: 19 percent / triethylamine / CHCl3 / 2 h / Heating 2: tert-butyl hypochlorite / CH2Cl2 / 5 h 3: 57 percent / acetone / Ambient temperature View Scheme
参考文献
Campbell, John J.; Glover, Stephen A.; Hammond, Gerard P.; Rowbottom, Colleen A.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1991 , # 12 p. 2067 - 2080
1: 76 percent / K2CO3; NaI / dimethylformamide / 6 h / 20 °C 2: 97 percent / aq. KOH / dioxane / 1 h 3: 1-chloro-2,N,N-trimethylprop-1-en-1-ylamine / tetrahydrofuran / 40 h / -18 °C 4: 0.16 g / Fe(acac)3 / tetrahydrofuran / 0.5 h / 0 °C View Scheme
参考文献
Fuerstner, Alois; De Souza, Dominic; Turet, Laurent; Fenster, Michael D. B.; Parra-Rapado, Liliana; Wirtz, Conny; Mynott, Richard; Lehmann, Christian W.
Chemistry - A European Journal, 2007 , vol. 13, # 1 p. 115 - 134
1: 1-Bromo-2-aminobenzene With n-butyllithium in tetrahydrofuran T=-78°C; 0.166667 h; 2: p-methoxybenzyl chloride in tetrahydrofuran T=-78°C; 0.333333 h; Further stages.;
参考文献
Reisman, Sarah E.; Ready, Joseph M.; Weiss, Matthew M.; Hasuoka, Atsushi; Hirata, Makoto; Tamaki, Kazuhiko; Ovaska, Timo V.; Smith, Catherine J.; Wood, John L.
Journal of the American Chemical Society, 2008 , vol. 130, # 6 p. 2087 - 2100
