1.1: t-BuOK; BuLi / hexane; tetrahydrofuran / 2 h / -95 °C
1.2: ClSnBu3 / hexane; tetrahydrofuran / 2 h / -95 - -50 °C
1.3: 0.45 g / Pd(PPh3)4 / CHCl3 / 2 h / 60 °C
2.1: 74 percent / Amberlyst-15 / CH2Cl2 / 1 h / 25 °C
View Scheme
参考文献
Tivola, Paolo Balma; Deagostino, Anna; Prandi, Cristina; Venturello, Paolo
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 4 p. 437 - 441