hydrogenchloride in diethyl ether; water; pentane T=-20°C; Inert atmosphereReflux;
参考文献
Van Zandt, Michael C.; Doan, Brian; Sawicki, Diane R.; Sredy, Janet; Podjarny, Alberto D.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 7 p. 2006 - 2008
1: With tert.-butyl lithium in diethyl ether; pentane
T=-78 - -30°C; 5 h; Inert atmosphere;
2: With N,N-dimethyl-formamide in diethyl ether; pentane
T=-30°C; 0.166667 h; Inert atmosphere;
参考文献
Van Zandt, Michael C.; Doan, Brian; Sawicki, Diane R.; Sredy, Janet; Podjarny, Alberto D.
Bioorganic and Medicinal Chemistry Letters, 2009 , vol. 19, # 7 p. 2006 - 2008
