您好，欢迎来到魔法化学网！
合作交流
|
服务时间(9:30-18:00)
百科
百科
▼
百科
资讯
搜索
结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
首页
化合物百科
价格行情
资讯
化工导航
实验室工具
搜索
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82589-56-8
合成路线
（共 5 条）
82589-42-2
→
反应条件
82589-56-8
反应条件
1: 69.5 percent / Heating 2: POCl3 / toluene / 95 °C 3: NaBH4 / methanol / Ambient temperature View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
66-77-3
1-萘甲醛
→
反应条件
82589-56-8
反应条件
1: 78 percent / piperidine acetate / toluene / Heating 2: 92 percent / LiAlH4 / tetrahydrofuran / Heating 3: 50percent aq. sulphuric acid / a. water removed, b. 130-140 deg C (15mm), 2h 4: 10percent aq. NaOH / Heating 5: 69.5 percent / Heating 6: POCl3 / toluene / 95 °C 7: NaBH4 / methanol / Ambient temperature View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
82590-45-2
→
反应条件
82589-56-8
反应条件
1: 50percent aq. sulphuric acid / a. water removed, b. 130-140 deg C (15mm), 2h 2: 10percent aq. NaOH / Heating 3: 69.5 percent / Heating 4: POCl3 / toluene / 95 °C 5: NaBH4 / methanol / Ambient temperature View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
82589-50-2
→
反应条件
82589-56-8
反应条件
1: POCl3 / toluene / 95 °C 2: NaBH4 / methanol / Ambient temperature View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
82590-37-2
→
反应条件
82589-56-8
反应条件
1: 92 percent / LiAlH4 / tetrahydrofuran / Heating 2: 50percent aq. sulphuric acid / a. water removed, b. 130-140 deg C (15mm), 2h 3: 10percent aq. NaOH / Heating 4: 69.5 percent / Heating 5: POCl3 / toluene / 95 °C 6: NaBH4 / methanol / Ambient temperature View Scheme
参考文献
Gaur, S. P.; Jain, Padam C.; Anand, Nitya
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 1 p. 46 - 51
