1-甲基-3,4-二氢-1H-喹啉-2-酮合成路线 （共 34 条）
反应条件
hydrogen in methanol
T=20°C; 3 h; Schlenk technique;
参考文献
Liu, Baoqing; Fan, Yang; Gao, Yang; Sun, Chao; Xu, Cheng; Zhu, Jin
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 468 - 473
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in dimethyl sulfoxide
T=120°C; 36 h;
参考文献
Zhou, Wang; Zhang, Liangren; Jiao, Ning
Tetrahedron, 2009 , vol. 65, # 10 p. 1982 - 1987
反应条件
sodium hydride in tetrahydrofuran; N,N-dimethyl-formamide
参考文献
Ohbayashi, Tohru; Mitsunaga, Shintaro; Satoh, Tsuyoshi
Tetrahedron Letters, 2007 , vol. 48, # 44 p. 7829 - 7833
反应条件
sulfur dioxide in water
T=130 - 140°C; 70 h;
参考文献
Ignatchenko, A. V.; Terent'ev, P. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 292 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 348 - 351
反应条件
potassium permanganate in acetonitrile
2 h; Ambient temperature;
参考文献
Venkov; Statkova-Abeghe
Tetrahedron, 1996 , vol. 52, # 4 p. 1451 - 1460
反应条件
hydrogen; nickel
P=760 Torr;
参考文献
Collins, Christopher J.; Lanz, Marc; Singaram, Bakthan
Tetrahedron Letters, 1999 , vol. 40, # 19 p. 3673 - 3676
反应条件
sulfur dioxide in water
T=150°C; 90 h; sealed ampul; other time (40 h), other temp. (140-150 deg C);
参考文献
Ignatchenko, A. V.; Terent'ev, P. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 292 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 348 - 351
反应条件
sulfur dioxide in water
T=150°C; 14 h;
参考文献
Ignatchenko, A. V.; Terent'ev, P. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 292 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 348 - 351
反应条件
sulfur dioxide in water
T=150°C; 14 h; sealed ampul;
参考文献
Ignatchenko, A. V.; Terent'ev, P. B.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 3 p. 292 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , vol. 23, # 3 p. 348 - 351
反应条件
1: silver(I) acetate; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; silver hexafluoroantimonate / methanol / 12 h / 35 °C
2: hydrogen / methanol / 3 h / 20 °C / |Schlenk technique
View Scheme
参考文献
Liu, Baoqing; Fan, Yang; Gao, Yang; Sun, Chao; Xu, Cheng; Zhu, Jin
Journal of the American Chemical Society, 2013 , vol. 135, # 1 p. 468 - 473
