1.1: copper(l) chloride; sodium t-butanolate / tetrahydrofuran / 0.17 h / 20 °C 1.2: 20 - 65 °C 2.1: potassium tert-butylate / diethyl ether / -45 °C / 760.05 Torr View Scheme
参考文献
Grigg, R. David; Rigoli, Jared W.; Van Hoveln, Ryan; Neale, Samuel; Schomaker, Jennifer M.
Chemistry - A European Journal, 2012 , vol. 18, # 30 p. 9391 - 9396
1: With benzo[1,3,2]dioxaborole; rhodium complex 2 in toluene T=20°C; Addition; Hydroboration; 2 h; 2: With sodium hydroxide; water; dihydrogen peroxide in toluene T=20°C; Oxidation; 2 h; Title compound not separated from byproducts;
参考文献
Doucet, Henri; Fernandez, Elena; Layzell, Timothy P.; Brown, John M.
Chemistry - A European Journal, 1999 , vol. 5, # 4 p. 1320 - 1330
