4-(三甲基硅基)-1H-吲哚合成路线 （共 6 条）
反应条件
in methanol Heating;
参考文献
Barrett, Anthony G. M.; Dauzonne, Daniel; Williams, David J.
Journal of the Chemical Society, Chemical Communications, 1982 , # 11 p. 636 - 637
反应条件
1: 1.)n-BuLi / 1.) THF, -20 deg C, 1 h; 2.) YHF, -20 deg C, 1 h View Scheme
参考文献
Tetrahedron, , vol. 44, # 23 p. 7325 - 7334
反应条件
1: 1.) lithium metal, 2.) p-benzoquinone / 1.) THF, 5 to 45 deg C, 2.) CH2Cl2, 0 deg C 2: 94 percent / methanol / Heating View Scheme
参考文献
Journal of the Chemical Society, Chemical Communications, , # 11 p. 636 - 637
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 44, # 23 p. 7325 - 7334
反应条件
sodium hydride
1) 20-40 deg C, THF, 2) THF, -78 deg C, 3) room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Barrett, Anthony G. M.; Dauzonne, Daniel; Williams, David J.
Journal of the Chemical Society, Chemical Communications, 1982 , # 11 p. 636 - 637
反应条件
1: NaH / 1) 20-40 deg C, THF, 2) THF, -78 deg C, 3) room temperature, 1 h
2: 46 percent / AlCl3 / CH2Cl2 / 15 h / Ambient temperature
View Scheme
参考文献
Barrett, Anthony G. M.; Dauzonne, Daniel; O'Neil, Ian A.; Renaud, Alain
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4409 - 4415
