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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
82657-70-3
合成路线
（共 13 条）
82657-70-3
→
反应条件
3166-97-0
反应条件
thionyl chloride; sodium hydrogencarbonate in chloroform; water
参考文献
Hanabata, Makoto; Sato, Masahiro; Katayama, Junko; Kitajima, Satsuki; Niwa, Atsushi
Patent: US2003/211421 A1, 2003 ;
82657-70-3
→
反应条件
26114-12-5
4-丙基苯乙酸
反应条件
1: triethylamine / dichloromethane / 0.5 h / 0 °C / |Inert atmosphere 2: sodium iodide / acetone / 0.25 h / 20 °C 3: N,N-dimethyl-formamide / 2 h / 20 °C / |Inert atmosphere 4: sodium hydroxide; water / 4 h / |Reflux View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1360803-32-2
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反应条件
82657-70-3
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran T=0°C; 0.5 h; Inert atmosphere;
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
Location in patent: Paragraph 0087; 0088 ;
28785-06-0
4-丙基苯甲醛
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反应条件
82657-70-3
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0°C; 2 h;
参考文献
Sundaresan, Arun Kumar; Ramamurthy
Organic Letters, 2007 , vol. 9, # 18 p. 3575 - 3578
2438-05-3
4-丙基苯甲酸
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反应条件
82657-70-3
反应条件
lithium aluminium tetrahydride in diethyl ether Reduction; 1 h; Heating;
参考文献
Chen, Guangping; Banoglu, Erden; Duffel, Michael W.
Chemical Research in Toxicology, 1996 , vol. 9, # 1 p. 67 - 74
52710-27-7
4-丙基苯甲酰氯
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反应条件
82657-70-3
反应条件
sodium tetrahydroborate in tetrahydrofuran T=0°C; 2 h;
参考文献
Sundaresan, Arun Kumar; Ramamurthy
Organic Letters, 2007 , vol. 9, # 18 p. 3575 - 3578
1093190-16-9
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反应条件
82657-70-3
反应条件
1.1: potassium carbonate; methanol / 2 h / 20 °C / |Inert atmosphere 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 2.2: 0.5 h / 20 °C / |Inert atmosphere 3.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
275386-60-2
4-(三甲基硅基乙炔基)苄基甲醇
→
反应条件
82657-70-3
反应条件
1.1: 1H-imidazole / tetrahydrofuran / 15 h / 0 - 20 °C / |Inert atmosphere 2.1: potassium carbonate; methanol / 2 h / 20 °C / |Inert atmosphere 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 3.2: 0.5 h / 20 °C / |Inert atmosphere 4.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1093190-17-0
→
反应条件
82657-70-3
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / |Inert atmosphere 1.2: 0.5 h / 20 °C / |Inert atmosphere 2.1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
1360803-31-1
→
反应条件
82657-70-3
反应条件
1: hydrogen; palladium 10 on activated carbon / ethyl acetate / 15001.5 Torr 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C / |Inert atmosphere View Scheme
参考文献
Postech Academy-industry Foundation; SHIN, Seung Koo; YOON, Hye Joo; JUNG, Yong Sik; LEE, Hee Yoon; SUH, Min Soo; SEO, Jong Cheol
Patent: EP2610243 A2, 2013 ;
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