Boc-Lysinol(Z)合成路线 (共 4 条)
反应条件
1: With 1-propanephosphonic acid cyclic anhydride; N-ethyl-N,N-diisopropylamine in ethyl acetate
T=0°C; 0.166667 h;
2: With sodium tetrahydroborate in water; ethyl acetate
T=0°C; 0.583333 h;
参考文献
Nagendra; Madhu; Vishwanatha; Sureshbabu, Vommina V.
Tetrahedron Letters, 2012 , vol. 53, # 38 p. 5059 - 5063
反应条件
sodium borohydride; lithium chloride in tetrahydrofuran; ethanol; water
参考文献
Carry, Jean-Christophe; Damour, Dominique; Guyon, Claude; Mignani, Serge; Bigot, Antony; Bacque, Eric; Tabart, Michel
Patent: US2002/22631 A1, 2002 ;
反应条件
sodium tetrahydroborate in ethylene glycol dimethyl ether; water
T=-15°C; 0.00833333 h; Yield given;
参考文献
Rodriguez; Llinares; Doulut; Heitz; Martinez
Tetrahedron Letters, 1991 , vol. 32, # 7 p. 923 - 926
反应条件
sodium tetrahydroborate; lithium chloride in tetrahydrofuran; ethanol
参考文献
Hamada; Shioiri
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1921 - 1924