lithium aluminium tetrahydride in tetrahydrofuran
T=20°C; 15 h;
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: Et3N / CH2Cl2 / 72 h / 20 °C
2: 96 percent / K2CO3 / methanol / 1 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: Et3N / CH2Cl2 / 72 h / 20 °C
2: 96 percent / K2CO3 / methanol / 1 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: phosphorus pentasulfide
2: tetrahydrofuran / 17 h / 0 °C
3: Et3N / CH2Cl2 / 72 h / 20 °C
4: 94 percent / LiAlH4 / tetrahydrofuran / 15 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: tetrahydrofuran / 17 h / 0 °C
2: Et3N / CH2Cl2 / 72 h / 20 °C
3: 94 percent / LiAlH4 / tetrahydrofuran / 15 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: phosphorus pentasulfide
2: tetrahydrofuran / 1 h / 0 °C
3: Et3N / CH2Cl2 / 72 h / 20 °C
4: 96 percent / K2CO3 / methanol / 1 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
1: tetrahydrofuran / 1 h / 0 °C
2: Et3N / CH2Cl2 / 72 h / 20 °C
3: 96 percent / K2CO3 / methanol / 1 h / 20 °C
View Scheme
参考文献
Michael, Joseph P.; De Koning, Charles R.; Malefetse, Tshepo J.; Yillah, Ibrahim
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 23 p. 3510 - 3517
