α-N,N-二甲氨基苯乙腈合成路线 (共 42 条)
反应条件
water; sodium hydrogensulfite anschliessend Behandeln mit Natriumcyanid;
参考文献
Journal of Organic Chemistry, , vol. 3, p. 590,594
Organic Syntheses, , vol. 43, p. 25
反应条件
1: diethyl ether / Ambient temperature 2: dioxane; methanol / 30 h / Ambient temperature View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 40, p. 939 - 941
反应条件
in 1,4-dioxane; methanol 30 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 40, p. 939 - 941
反应条件
methyllithium; titanium tetrachloride 1.) THF, 0 deg C; 2.) CH2Cl2, -78 deg C, 30 min, -78 deg C, then Rt, 10 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 241 - 242
反应条件
in methanol; water 4 h; Ambient temperature; Yield given;
参考文献
Synthesis, , # 2 p. 109 - 110
反应条件
T=50°C; 15 h; Mechanism;
参考文献
Liebigs Annalen der Chemie, , # 3 p. 358 - 371
反应条件
(i) NaHSO3, H2O, (ii) /BRN= 605257/, (iii) /BRN= 3587243/; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 2319 - 2324
参考文献
Chemische Berichte, , vol. 104, p. 932 - 940
反应条件
Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 61, # 3 p. 735 - 740
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; oxygen in dimethyl sulfoxide 3 h;
参考文献
Yuste, Francisco; Origel, Alfredo E.; Brena, Leonardo J.
Synthesis, 1983 , # 2 p. 109 - 110