(4R)-6-甲基-4-苯基色满-2-酮合成路线 (共 12 条)
反应条件
1.1: calcium carbonate; palladium diacetate / methanol / 4 h / 60 °C
1.2: 20 °C
2.1: copper diacetate; DEMS; josiphos / tetrahydrofuran; toluene; tert-butyl alcohol / 3 h / 20 °C / |Inert atmosphere
3.1: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Barancelli, Daniela A.; Salles, Airton G.; Taylor, Jason G.; Correia, Carlos Roque D.
Organic Letters, 2012 , vol. 14, # 23 p. 6036 - 6039
反应条件
1: copper diacetate; DEMS; josiphos / tetrahydrofuran; toluene; tert-butyl alcohol / 3 h / 20 °C / |Inert atmosphere
2: pyridinium chlorochromate / dichloromethane / 3 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Barancelli, Daniela A.; Salles, Airton G.; Taylor, Jason G.; Correia, Carlos Roque D.
Organic Letters, 2012 , vol. 14, # 23 p. 6036 - 6039