反应条件
1: With triethylamine; 4-(N,N-dimethlyamino)pyridine in DMF (N,N-dimethyl-formamide); toluene
T=20°C; 19 h;
2: With ammonium acetate in DMF (N,N-dimethyl-formamide); toluene
T=90°C; 5 h;
参考文献
MYRIAD GENETICS, INC.; CYTOVIA, INC.
Patent: WO2006/74187 A2, 2006 ;
Location in patent: Page/Page column 59 ;
WO 2006/074187 A2
