(7S)-7-(二丙基氨基)-5,6,7,8-四氢-2-萘酚氢溴酸盐(1:1)合成路线 (共 3 条)
反应条件
boron tribromide in dichloromethane
Ambient temperature;
参考文献
Wikstroem, Hakan; Andersson, Bengt; Sanchez, Domingo; Lindberg, Per; Arvidsson, Lars-Erik; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 2 p. 215 - 225
反应条件
1: 90 percent / LiAlH4 / diethyl ether
2: BBr3 / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Wikstroem, Hakan; Andersson, Bengt; Sanchez, Domingo; Lindberg, Per; Arvidsson, Lars-Erik; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 2 p. 215 - 225
反应条件
1: 100 percent / 5percent aq. NaOH / CH2Cl2 / 0.5 h
2: 90 percent / LiAlH4 / diethyl ether
3: BBr3 / CH2Cl2 / Ambient temperature
View Scheme
参考文献
Wikstroem, Hakan; Andersson, Bengt; Sanchez, Domingo; Lindberg, Per; Arvidsson, Lars-Erik; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 2 p. 215 - 225