3-(2-溴苯基)-5-苯基-1,2,4-噁二唑合成路线 （共 4 条）
反应条件
potassium phosphate; oxygen in N,N-dimethyl-formamide T=60°C; P=760.051 Torr; 10 h;
参考文献
Zhang, Feng-Lian; Wang, Yi-Feng; Chiba, Shunsuke
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 36 p. 6003 - 6007
反应条件
1: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C / |Inert atmosphere 2: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / |Inert atmosphere 3: potassium phosphate; oxygen / N,N-dimethyl-formamide / 10 h / 60 °C / 760.05 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
反应条件
1: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / |Inert atmosphere 2: potassium phosphate; oxygen / N,N-dimethyl-formamide / 10 h / 60 °C / 760.05 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
反应条件
1: hydroxylamine hydrochloride; sodium acetate / ethanol 2: N-chloro-succinimide / N,N-dimethyl-formamide / 4 h / 20 °C / |Inert atmosphere 3: triethylamine / N,N-dimethyl-formamide / 6 h / 0 - 20 °C / |Inert atmosphere 4: potassium phosphate; oxygen / N,N-dimethyl-formamide / 10 h / 60 °C / 760.05 Torr View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 36 p. 6003 - 6007
