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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
827340-35-2
合成路线
（共 12 条）
1375488-05-3
→
反应条件
827340-35-2
反应条件
ammonium cerium (IV) nitrate in water; acetonitrile T=20°C; 2 h; Inert atmosphere;
参考文献
Bhosale, Shrikar M.; Momin, Aadil A.; Kunjir, Shrikant; Rajamohanan; Kusurkar, Radhika S.
Tetrahedron Letters, 2014 , vol. 55, # 1 p. 155 - 162
827340-34-1
→
反应条件
827340-35-2
反应条件
tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=60°C;
参考文献
Sissouma, Drissa; Maingot, Lucie; Collet, Sylvain; Guingant, Andre
Journal of Organic Chemistry, 2006 , vol. 71, # 22 p. 8384 - 8389
1375488-00-8
→
反应条件
827340-35-2
反应条件
1: copper(l) iodide / methanol; N,N-dimethyl-formamide / 10 h / 120 °C / Inert atmosphere 2: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 3: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 4: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 5: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
1375487-97-0
→
反应条件
827340-35-2
反应条件
1.1: N-bromosuccinmide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere 2.2: 1 h / 20 °C / Inert atmosphere 3.1: copper(l) iodide / methanol; N,N-dimethyl-formamide / 10 h / 120 °C / Inert atmosphere 4.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 5.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 6.1: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 7.1: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
1375487-99-2
→
反应条件
827340-35-2
反应条件
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere 1.2: 1 h / 20 °C / Inert atmosphere 2.1: copper(l) iodide / methanol; N,N-dimethyl-formamide / 10 h / 120 °C / Inert atmosphere 3.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 4.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 5.1: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 6.1: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
1375488-02-0
→
反应条件
827340-35-2
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 2: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 3: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 4: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
1375488-03-1
→
反应条件
827340-35-2
反应条件
1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 2: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 3: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
1375488-04-2
→
反应条件
827340-35-2
反应条件
1: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 2: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
615-43-0
2-碘苯胺
→
反应条件
827340-35-2
反应条件
1: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 2: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 3: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 4: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
52602-39-8
4-羟基咔唑
→
反应条件
827340-35-2
反应条件
1.1: trichlorophosphate / 10 - 20 °C / Inert atmosphere 1.2: 20 - 35 °C / Inert atmosphere 1.3: 30 °C / Cooling with ice; Inert atmosphere 2.1: N-bromosuccinmide / N,N-dimethyl-formamide / 20 °C / Inert atmosphere 3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 - 20 °C / Inert atmosphere 3.2: 1 h / 20 °C / Inert atmosphere 4.1: copper(l) iodide / methanol; N,N-dimethyl-formamide / 10 h / 120 °C / Inert atmosphere 5.1: toluene-4-sulfonic acid / tetrahydrofuran / 0.25 h / Reflux; Inert atmosphere 6.1: triethylamine / dichloromethane / 2 h / 20 °C / Inert atmosphere 7.1: palladium diacetate; potassium carbonate; triphenylphosphine / N,N-dimethyl-formamide / 7 h / 120 °C / Inert atmosphere 8.1: ammonium cerium (IV) nitrate / water; acetonitrile / 2 h / 20 °C / Inert atmosphere View Scheme
参考文献
Bhosale, Shrikar M.; Gawade, Rupesh L.; Puranik, Vedavati G.; Kusurkar, Radhika S.
Tetrahedron Letters, 2012 , vol. 53, # 23 p. 2894 - 2896
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