(S)-3-二甲基氨基-3-苯丙醇合成路线 (共 13 条)
反应条件
1: ethyl acetate; ethanol / 1 h / 30 °C / Reflux 2: caustic lye / dichloromethane; water / 0.5 h / 20 °C / pH 9 - 10 View Scheme
反应条件
1.1: sodium tetrahydroborate / tetrahydrofuran 1.2: 30 °C 1.3: pH 9 - 10 2.1: ethanol; acetone / 30 - 58 °C 3.1: caustic lye / dichloromethane; water / 0.17 h / 20 °C View Scheme
反应条件
1.1: potassium tert-butylate / dimethyl sulfoxide / 3 h / 90 °C 1.2: 30 °C / pH ~ 1 1.3: caustic lye / pH ~ 9 2.1: ethanol; acetone / 30 - 58 °C 3.1: caustic lye / dichloromethane; water / 0.17 h / 20 °C View Scheme