2-碘-1,1:3,1-三联苯合成路线 （共 19 条）
反应条件
copper T=260 - 270°C; 3 h; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 5 p. 1572 - 1581
反应条件
magnesium in diethyl ether; benzene 3 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 3 p. 802 - 809
反应条件
copper T=260 - 270°C; 3 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 5 p. 1572 - 1581
反应条件
copper T=260 - 270°C; 3 h; Further byproducts given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 5 p. 1572 - 1581
反应条件
bis(acetylacetonate)nickel(II) 1.) reflux, 3h; 2.) hydrochloric acid; Yield given. Multistep reaction;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 5 p. 1572 - 1581
反应条件
iodine in tetrahydrofuran
T=20°C;
参考文献
Gallego, Daniel; Brueck, Andreas; Irran, Elisabeth; Meier, Florian; Kaupp, Martin; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 41 p. 15617 - 15626
反应条件
1: copper powder / 1.) 185-190 deg C, 3 h; 2.) 210-220 deg C, 1 h
2: 95 percent / activated iron, hydrogen chloride / benzene
3: 1.) sodium nitrite, concenrated sulfuric acid; 2.) potassium iodide
View Scheme
参考文献
Ozasa, Shigeru; Fujioka, Yasuhiro; Kikutake, Jun-ichiro; Ibuki, Eiichi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1572 - 1581
反应条件
1: 95 percent / activated iron, hydrogen chloride / benzene
2: 1.) sodium nitrite, concenrated sulfuric acid; 2.) potassium iodide
View Scheme
参考文献
Ozasa, Shigeru; Fujioka, Yasuhiro; Kikutake, Jun-ichiro; Ibuki, Eiichi
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1572 - 1581
反应条件
1: diethyl ether / 15 h / 20 °C
2: iodine / tetrahydrofuran / 20 °C
View Scheme
参考文献
Gallego, Daniel; Brueck, Andreas; Irran, Elisabeth; Meier, Florian; Kaupp, Martin; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 41 p. 15617 - 15626
反应条件
1: diethyl ether / 15 h / 20 °C
2: iodine / tetrahydrofuran / 20 °C
View Scheme
参考文献
Gallego, Daniel; Brueck, Andreas; Irran, Elisabeth; Meier, Florian; Kaupp, Martin; Driess, Matthias; Hartwig, John F.
Journal of the American Chemical Society, 2013 , vol. 135, # 41 p. 15617 - 15626
