反应条件
water; ammonium chloride in hexane
byproducts: LiNMe2; in sealed evacuated ampule; in the course of 0.5 h at room temp. amide added to soln. of Et3GeLi; stirred for 4 h; hydrolized with satd. NH4Cl; dried; org. part solvent removed under reduced pressure; products isolated by fractionation; GLC; PMR; mass-spectrometry; elem. anal.;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60