暂无反应条件数据

1: triethylamine / H2O / 5 h / 70 °C 2: 34.7 g / pyridine / 5 h / Ambient temperature 3: 87 percent / diphenyl phosphorochloridate / pyridine / 3 h / Ambient temperature 4: triethylamine / acetonitrile / 1 h / Ambient temperature 5: methanolic sodium methoxide / 0.25 h / Ambient temperature View Scheme

1: 34.7 g / pyridine / 5 h / Ambient temperature 2: 87 percent / diphenyl phosphorochloridate / pyridine / 3 h / Ambient temperature 3: triethylamine / acetonitrile / 1 h / Ambient temperature 4: methanolic sodium methoxide / 0.25 h / Ambient temperature View Scheme

1: triethylamine / acetonitrile / 1 h / Ambient temperature 2: methanolic sodium methoxide / 0.25 h / Ambient temperature View Scheme

1: diphenyl carbonate, sodium hydrogen carbonate / hexamethylphosphoric acid triamide / 0.33 h / 150 °C 2: triethylamine / H2O / 5 h / 70 °C 3: 34.7 g / pyridine / 5 h / Ambient temperature 4: 87 percent / diphenyl phosphorochloridate / pyridine / 3 h / Ambient temperature 5: triethylamine / acetonitrile / 1 h / Ambient temperature 6: methanolic sodium methoxide / 0.25 h / Ambient temperature View Scheme

1: 87 percent / diphenyl phosphorochloridate / pyridine / 3 h / Ambient temperature 2: triethylamine / acetonitrile / 1 h / Ambient temperature 3: methanolic sodium methoxide / 0.25 h / Ambient temperature View Scheme

1: 57 percent 2: 91 percent View Scheme