反应条件
1.1: 81 percent / p-toluenesulfonic acid monohydrate; MeOH / 56 h / Heating
2.1: NaH / tetrahydrofuran / 0 °C
2.2: tetrahydrofuran / 20 °C
3.1: LiAlH4 / diethyl ether / 20 °C
4.1: NaH / tetrahydrofuran; dimethylformamide / 0 °C
4.2: tetrahydrofuran; dimethylformamide / 20 °C
5.1: aq. trifluoroacetic acid / CHCl3 / 20 °C
View Scheme
参考文献
Shintani, Ryo; Okamoto, Kazuhiro; Otomaru, Yusuke; Ueyama, Kazuhito; Hayashi, Tamio
Journal of the American Chemical Society, 2005 , vol. 127, # 1 p. 54 - 55
