2,4-二甲氧基苯乙酮合成路线 (共 100 条)
反应条件
1: 1.) room temperature, 3 h, 2.) 0 deg C, 17 h 2: 92 percent / H2O / 0.17 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 5 p. 1075 - 1082
反应条件
1: NaOH 2: 75 percent / SmI3 / acetonitrile / 2 h / 20 °C View Scheme
参考文献
Journal of Chemical Research, , # 2 p. 80 - 81
反应条件
bromine in chloroform
参考文献
European Journal of Medicinal Chemistry, , vol. 65, p. 102 - 111
反应条件
1: palladium (II) trifluoroacetate; 6-mbipy; p-benozquinone / N,N-dimethyl-formamide / 24 h / 120 °C 2: hydrogenchloride; water / 2 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 356, # 4 p. 870 - 878
反应条件
1: sodium hydroxide / water / 3 h / 0 - 70 °C 2: AlCl3, aluminium chloride / dichloromethane / 1 h / 0 - 20 °C View Scheme
参考文献
Synthetic Communications, , vol. 44, # 4 p. 540 - 546
反应条件
methanol; potassium hydroxide
参考文献
Chemische Berichte, , vol. 24, p. 2461
反应条件
hydrogenchloride; diethyl ether und Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Yakugaku Zasshi, , p. 111
Chem. Zentralbl., , vol. 99, # I p. 333
反应条件
9,10-dihydro-anthracene in diphenylether T=219.85 - 299.85°C; competition reaction with α-phenoxyacetophenone; Product distribution;
参考文献
European Journal of Organic Chemistry, , # 3 p. 607 - 616
反应条件
potassium tert-butylate; palladium dichloride; α,α'-bis(di-t-butylphosphino)-o-xylene T=100°C; 48 h; Further byproducts given;
参考文献
Dalton Transactions, , # 10 p. 1826 - 1830
参考文献
Monatshefte fuer Chemie, , vol. 15, p. 438
Chemische Berichte, , vol. 28, p. 2306