9-芴甲基-N-琥珀酰亚胺基碳酸酯合成路线 （共 303 条）
反应条件
sodium carbonate in water; acetone T=20°C; 20 h; enantioselective reaction;
参考文献
Reyes-Rangel, Gloria; Jimenez-Gonzalez, Erika; Olivares-Romero, Jose Luis; Juaristi, Eusebio
Tetrahedron Asymmetry, 2008 , vol. 19, # 24 p. 2839 - 2849
反应条件
1.1: sodium carbonate / tetrahydrofuran; water / 48 h 1.2: pH 2 - 3 2.1: thionyl chloride / dichloromethane / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron Asymmetry, , vol. 22, # 6 p. 613 - 618
反应条件
1.1: aq. NaHCO3 / dioxane / 0.5 h / 20 °C 1.2: 97 percent / dioxane / 24 h / 20 °C 2.1: 92 percent / 4-dimethylaminopyridine; pyridine / 16 h / -5 °C 3.1: 84 percent / NaI / acetone / 48 h / 20 °C View Scheme
参考文献
Shao, Hui; Lockman, Jeffrey W.; Parquette, Jon R.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1884 - 1885
反应条件
triethylamine in N,N-dimethyl-formamide; acetonitrile
参考文献
Kuil, Joeri; van Wandelen, Loek T.M.; de Mol, Nico J.; Liskamp, Rob M.J.
Bioorganic and Medicinal Chemistry, 2008 , vol. 16, # 3 p. 1393 - 1399
反应条件
1: Nδ-Boc-L-ornithine With N,N-dicyclohexylamine in acetone T=20°C; 2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione With sodium carbonate in water; acetonitrile T=0 - 20°C; pH=8; 3: With potassium hydrogensulfate in water; acetonitrile pH=2 - 3;
参考文献
Nowshuddin, Shaik; Rao; Reddy, A. Ram
Synthetic Communications, 2009 , vol. 39, # 11 p. 2022 - 2031
反应条件
1: di-tert-butyl dicarbonate; L-(+)-ornithine hydrochloride With sodium hydroxide; copper diacetate in water; acetone 44 h; 2: With 8-hydroxy-quinoline; sodium carbonate in water; acetone 1.5 h; 3: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione in water; acetone 1.5 h;
参考文献
Masiukiewicz, Elzbieta; Wiejak, Stanislaw; Rzeszotarska, Barbara
Organic Preparations and Procedures International, 2002 , vol. 34, # 5 p. 531 - 537
反应条件
1: With sodium carbonate in water; acetonitrile T=0 - 20°C; pH=8; 2: With potassium hydrogensulfate in water; acetonitrile pH=2 - 3;
参考文献
Nowshuddin, Shaik; Rao; Reddy, A. Ram
Synthetic Communications, 2009 , vol. 39, # 11 p. 2022 - 2031
反应条件
1: sodium carbonate / acetone 2: thionyl chloride / dichloromethane View Scheme
参考文献
Chen, Laizhong; Li, Jing; Liu, Zhenzhen; Ma, Zhao; Zhang, Wei; Du, Lupei; Xu, Wenfang; Fang, Hao; Li, Minyong
RSC Advances, 2013 , vol. 3, # 32 p. 13412 - 13416
反应条件
1: With sodium carbonate in water; acetonitrile T=0 - 20°C; pH=8; 2: With potassium hydrogensulfate in water; acetonitrile pH=2 - 3;
参考文献
Synthetic Communications, , vol. 39, # 11 p. 2022 - 2031
反应条件
in 1,4-dioxane; water T=20°C; 16 h;
参考文献
Crestey, Francois; Ottesen, Lars K.; Jaroszewski, Jerzy W.; Franzyk, Henrik
Tetrahedron Letters, 2008 , vol. 49, # 41 p. 5890 - 5893
