9-芴甲基-N-琥珀酰亚胺基碳酸酯合成路线 （共 303 条）
反应条件
1: With water; sodium carbonate in 1,4-dioxane T=5 - 20°C; Cooling with ice; 2: With hydrogenchloride in 1,4-dioxane; water
参考文献
VALORISATION-RECHERCHE SOCIETE EN COMMANDITE; LUBELL, William; JAMIESON, Andrew; BOUTARD, Nicolas; RONGA, Luisa; ST-CYR, Daniel; TURCOTTE, Daniel; CHEN, Wang
Patent: WO2010/105367 A1, 2010 ;
Location in patent: Page/Page column 35; 36; 37 ;
反应条件
sodium hydroxide; sodium hydrogencarbonate
参考文献
Ho, Bin; Zabriskie, T. Mark
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 7 p. 739 - 744
反应条件
sodium carbonate in water; acetone
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 8 p. 1391 - 1394
反应条件
sodium hydrogencarbonate in water; acetone 3 h; Yield given;
参考文献
SCHERING CORPORATION
Patent: EP1135374 B1, 2006 ;
Location in patent: Page/Page column 24 ;
反应条件
sodium hydrogencarbonate in N,N-dimethyl-formamide; acetone T=20°C;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; GOODMAN, Zelda
Patent: WO2005/18682 A2, 2005 ;
Location in patent: Page/Page column 24-25 ;
WO 2005/018682 A2
反应条件
sodium hydrogencarbonate in 1,4-dioxane; water T=20°C; 2 h;
参考文献
Tetrahedron, , vol. 69, # 34 p. 7098 - 7101
反应条件
sodium hydroxide in 1,4-dioxane; water T=20°C; 0.25 h; Inert atmosphere;
参考文献
Heterocycles, , vol. 81, # 1 p. 79 - 89
反应条件
sodium carbonate in 1,4-dioxane; water 3 h;
参考文献
Patiny, Luc; Guichou, Jean-Francois; Keller, Michael; Turpin, Olivier; Rueckle, Thomas; Lhote, Philippe; Buetler, Timo M.; Ruegg, Urs T.; Wenger, Roland M.; Mutter, Manfred
Tetrahedron, 2003 , vol. 59, # 28 p. 5241 - 5249
反应条件
1.1: water; sodium carbonate / 1,4-dioxane / Cooling with ice 1.2: 20 °C / Cooling with ice 1.3: pH 3.5 2.1: tetrabutylammomium bromide; water; sodium hydrogencarbonate / dichloromethane / 20 h / 20 °C / Inert atmosphere View Scheme
参考文献
Wojnar, Joanna M.; Evans, Clive W.; Devries, Arthur L.; Brimble, Margaret A.
Australian Journal of Chemistry, 2011 , vol. 64, # 6 p. 723 - 731
参考文献
Wang, Jidong; Okada, Yoshio; Li, Wei; Yokoi, Toshio; Zhu, Jintao
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 5 p. 621 - 624
