9-芴甲基-N-琥珀酰亚胺基碳酸酯合成路线 （共 303 条）
反应条件
sodium carbonate in 1,4-dioxane
参考文献
Tetrahedron Letters, , vol. 49, # 33 p. 4958 - 4961
反应条件
triethylamine in acetonitrile 4 h; Ambient temperature;
参考文献
Muller, Dan; Zeltser, Irena; Bitan, Gal; Gilon, Chaim
Journal of Organic Chemistry, 1997 , vol. 62, # 2 p. 411 - 416
反应条件
sodium hydrogencarbonate in water; acetone Ambient temperature;
参考文献
Bo, Liu; Jiarong, Zhan
Synthetic Communications, 1999 , vol. 29, # 13 p. 2293 - 2299
反应条件
sodium hydroxide in 1,4-dioxane; water T=20°C; 72 h;
参考文献
ASTEX THERAPEUTICS LIMITED; THE INSTITUTE OF CANCER RESEARCH:ROYAL CANCER HOSPITAL; CANCER RESEARCH TECHNOLOGY LIMITED
Patent: WO2006/51290 A2, 2006 ;
Location in patent: Page/Page column 101-102 ;
WO 2006/051290 A2
反应条件
1: With sodium carbonate in 1,4-dioxane; water 2: With hydrogenchloride in 1,4-dioxane; water pH=3;
参考文献
Myriad Pharmaceuticals, Inc.
Patent: US2004/14763 A1, 2004 ;
Location in patent: Page 17; 18 ;
反应条件
sodium carbonate in acetone pH=9 - 10; 6 h;
参考文献
Schreiber, Juerg V.; Seebach, Dieter
Helvetica Chimica Acta, 2000 , vol. 83, # 12 p. 3139 - 3152
反应条件
1: With sodium hydrogencarbonate in water; acetone T=0°C; 23 h; 2: With water; acetic acid in ethyl acetate
参考文献
EP1135374 B1, ;
Page/Page column 33-34 ;
反应条件
sodium carbonate in 1,4-dioxane 3 h;
参考文献
Pearson, Daniel A.; Lister-James, John; McBride, William J.; Wilson, David M.; Martel, Lawrence J.; Civitello, Edgar R.; Taylor, John E.; Moyer, Brian R.; Dean, Richard T.
Journal of Medicinal Chemistry, 1996 , vol. 39, # 7 p. 1361 - 1371
反应条件
1.1: Na2CO3 / H2O / 12 h / 25 °C 1.2: H2O; dioxane / 4 h / 25 °C 1.3: 90 percent / citric acid / H2O; dioxane / pH 4 2.1: 85 percent / dithiothreitol / dimethylformamide; H2O / 4 h / 50 °C 3.1: 60 percent / trifluoroacetic acid / CH2Cl2 / 6 h / 25 °C View Scheme
参考文献
Jiang, Luyong; Burgess, Kevin
Tetrahedron, 2002 , vol. 58, # 43 p. 8743 - 8750
反应条件
sodium hydrogencarbonate in tetrahydrofuran; water T=20°C; 16 h; Inert atmosphere;
参考文献
Molecules, , vol. 15, # 3 p. 1590 - 1631
