9-芴甲基-N-琥珀酰亚胺基碳酸酯合成路线 （共 303 条）
反应条件
sodium carbonate in tetrahydrofuran; water T=20°C; pH=8 - 9; 18 h;
参考文献
Jin, Feng; Gao, Dan; Wu, Qin; Liu, Feng; Chen, Yuzong; Tan, Chunyan; Jiang, Yuyang
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 18 p. 5694 - 5706
反应条件
sodium carbonate in 1,4-dioxane; water T=0 - 20°C; 7.5 h;
参考文献
SANKARANARAYANAN, Alangudi
Patent: WO2005/33106 A1, 2005 ;
Location in patent: Page/Page column 61 ;
WO 2005/033106 A1
反应条件
1: 99 percent / N-ethyldiisopropylamine / CH2Cl2; H2O; dioxane 2: 97 percent / Dess-Martin periodinane / CH2Cl2 / 20 °C View Scheme
参考文献
Wessig, Pablo; Czapla, Sylvia; Moellnitz, Kristian; Schwarz, Jutta
Synlett, 2006 , # 14 p. 2235 - 2238
反应条件
1: (l)-serine methyl ester hydrochloride With sodium hydrogencarbonate in 1,4-dioxane T=20°C; 0.5 h; 2: 1-[[(9H-fluoren-9-ylmethoxy)carbonyl]oxy]-2,5-pyrrolidinedione in 1,4-dioxane T=20°C; 24 h;
参考文献
Shao, Hui; Lockman, Jeffrey W.; Parquette, Jon R.
Journal of the American Chemical Society, 2007 , vol. 129, # 7 p. 1884 - 1885
反应条件
sodium hydrogencarbonate in 1,4-dioxane 0.166667 h; Ambient temperature;
参考文献
Lapatsanis, Lucas; Milias, George; Froussios, Kleanthis; Kolovos, Miltiadis
Synthesis, 1983 , # 8 p. 671 - 673
反应条件
1: CH2Cl2 / 3.5 h / Ambient temperature 2: MeOH / CH2Cl2 / 0.5 h / Ambient temperature View Scheme
参考文献
Raillard, Stephen P.; Mann, Adam D.; Baer, Ted A.
Organic Preparations and Procedures International, 1998 , vol. 30, # 2 p. 183 - 186
反应条件
potassium carbonate in 1,4-dioxane; water T=23°C; 16 h;
参考文献
Tetrahedron, , vol. 63, # 28 p. 6577 - 6586
反应条件
sodium carbonate in acetone 12 h; Yield given;
参考文献
Koenig, Burkhard; Roedel, Martin
Synthetic Communications, 1999 , vol. 29, # 6 p. 943 - 949
反应条件
1: 77 percent / aq. NaHCO3 / acetone / Ambient temperature 2: 95 percent / DCC / ethyl acetate / 15 h / 0 °C View Scheme
参考文献
Djedaini-Pilard, Florence; Azaroual-Bellanger, Nathalie; Gosnat, Muriel; Vernet, Delphine; Perly, Bruno
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 4 p. 723 - 730
参考文献
Tossi, Alessandro; Benedetti, Fabio; Norbedo, Stefano; Skrbec, Damiano; Berti, Federico; Romeo, Domenico
Bioorganic and Medicinal Chemistry, 2003 , vol. 11, # 22 p. 4719 - 4727
